A price of molybdenum carbonyl bridge cyclohexyl mercaptan molybdenum and its synthesis

Cyclohexyl mercaptan monovalent Molybdenum tube molybdenum carbonyl bridge and its synthesis method involving chemical field, it is absolutely water anaerobic conditions, the Mo (CO) 6, C6H11Sna, Et4NCL reaction to synthesize a zero valence state molybdenum compound [Et4N ] 2 [Mo2 (SC6H11) 2 (CO) 8], the product 1; then the reaction product of 1 and the target product C6H11SNa [Et4N] [Mo2 (SC6H11) 3 (CO) 6], the product 2. The compound of the formula: C32H53Mo2NO6S3, formula weight: 835.81, unit cell parameters: a = 20.5805 (10) A, α = 90deg.b = 9.3127 (5) A, β = 90deg.c = 20.2955 (10) A , γ = 90deg. volume: 3889.8 (3) A3. Synthesis of the Compounds of molybdenum for the study of enzyme function and analog is meaningful. Its structure, may have some non-linear optical properties.
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